N-(4-溴苯基)吡啶-2-甲酰胺合成路线 (共 2 条)
反应条件
1: 2-pyridinecarboxylic acid chloride With triethylamine in dichloromethane T=0°C; 0.25 h; Inert atmosphere; 2: 4-bromo-aniline in dichloromethane T=0 - 20°C; 2.75 h; Inert atmosphere;
参考文献
Martinez, Angel Manu; Rodriguez, Nuria; Arrayas, Ramon Gomez; Carretero, Juan C.
Chemical Communications, 2014 , vol. 50, # 21 p. 2801 - 2803
反应条件
1.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 1.25 h / 0 °C / |Inert atmosphere 2.1: triethylamine / dichloromethane / 0.25 h / 0 °C / |Inert atmosphere 2.2: 2.75 h / 0 - 20 °C / |Inert atmosphere View Scheme
参考文献
Chemical Communications, , vol. 50, # 21 p. 2801 - 2803