1,4-二(十二烷氧基)-2,5-二碘苯合成路线 （共 12 条）
反应条件
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine in tetrahydrofuran
T=20°C; Sonogashira coupling; 24 h;
参考文献
Morisaki, Yasuhiro; Chujo, Yoshiki
Macromolecules, 2003 , vol. 36, # 25 p. 9319 - 9324
反应条件
1: 38 percent / Et3N; PdCl2(PPh3)2; CuI / tetrahydrofuran / 24 h / 40 °C
2: 42 percent / Et3N; PdCl2(PPh3)2; CuI / PPh3 / tetrahydrofuran / 24 h / 40 °C
3: 92 percent / n-Bu4NF / tetrahydrofuran / 16 h / 20 °C
View Scheme
参考文献
Morisaki, Yasuhiro; Chujo, Yoshiki
Macromolecules, 2003 , vol. 36, # 25 p. 9319 - 9324
