3,5-二氨基-1,2,4-三氮唑合成路线 （共 33 条）
反应条件
hydrogenchloride; potassium hydroxide; sodium nitrite in water 1.) from 0 to 5 deg C, 0.5 h, 2.) reflux;
参考文献
Kofman, T. P.; Uspenskaya, T. L.; Pevzner, M. S.
Russian Journal of Organic Chemistry, 1993 , vol. 29, # 11.2 p. 1942 - 1943
Zhurnal Organicheskoi Khimii, 1993 , vol. 29, # 11 p. 2328 - 2330
反应条件
in N,N-dimethyl-formamide 0.166667 h; Heating;
参考文献
Lipson; Desenko; Borodina; Shirobokova; Musatov
Russian Journal of Organic Chemistry, 2005 , vol. 41, # 1 p. 114 - 119
反应条件
in N,N-dimethyl-formamide 0.166667 h; Heating;
参考文献
Lipson; Desenko; Borodina; Shirobokova; Musatov
Russian Journal of Organic Chemistry, 2005 , vol. 41, # 1 p. 114 - 119
反应条件
in N,N-dimethyl-formamide 72 h; Ambient temperature;
参考文献
Hassan; Mohamed; Aly; Mourad
Die Pharmazie, 1997 , vol. 52, # 1 p. 23 - 28
反应条件
(1S)-10-camphorsulfonic acid in toluene T=100°C; 1.5 h; Heating / reflux;
参考文献
NIPPON KAYAKU KABUSHIKI KAISHA
Patent: EP1674454 A1, 2006 ;
Location in patent: Page/Page column 19 ;
反应条件
in not given molar ratio of indoline : triazole = 5:1; triturated with hot MeOH;
参考文献
Fernandez-Lazaro, Fernando; Sastre, Angela; Torres, Tomas
Journal of the Chemical Society, Chemical Communications, 1994 , # 13 p. 1525 - 1526
反应条件
1: 3,5-Diamino-1,2,4-triazole With sodium in methanol T=80 - 85°C; 1 h; Inert atmosphere; 2: dodecyl bromide in methanol 27 h; Inert atmosphereReflux;
参考文献
Wang, Mingfeng; Wudl, Fred
Journal of Materials Chemistry, 2010 , vol. 20, # 27 p. 5659 - 5663
参考文献
Fernandez-Lazaro, Fernando; Mendoza, Javier de; Mo, Otilia; Rodriguez-Morgade, Salome; Torres, Tomas; et al.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1989 , p. 797 - 804
反应条件
in acetic acid
Heating;
参考文献
Bishop, Brian C.; Marley, Hugh; Preston, Peter N.; Wright, Stanley H. B.
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 11 p. 1527 - 1532
参考文献
Ilford Ltd.
Patent: US2566658 , 1949 ;
