5,8-二羟基-2-甲基-1,4-萘醌合成路线 （共 6 条）
反应条件
aluminium trichloride in dichloromethane 2 h; Ambient temperature;
参考文献
Wurm, Gotthard; Goessler, Bernd
Archiv der Pharmazie (Weinheim, Germany), 1989 , vol. 322, p. 569 - 572
反应条件
aluminium trichloride; sodium chloride T=200 - 220°C;
参考文献
Eloeve, Guelnur A.; Schauble, J. Herman
Magnetic Resonance in Chemistry, 1987 , vol. 25, p. 194 - 200
反应条件
lead(IV) acetate; trifluoroacetic acid in benzene 24 h; Heating;
参考文献
Ogihara, Kazuhito; Yamashiro, Rieko; Higa, Matsutake; Yogi, Seiichi
Chemical and Pharmaceutical Bulletin, 1997 , vol. 45, # 3 p. 437 - 445
反应条件
2: 50 percent / SnCl4, Bu3N / toluene / 8 h / 60 °C 3: 1.) ClCOOEt, Et3N, 2.) NaBH4 / 1.) THF, 0 deg C, 1 h, 2.) THF, H2O, room temp., 12 h 4: 75 percent / Ce(IV)-ammonium nitrate / methanol; H2O; acetonitrile / 0.05 h / Ambient temperature 5: 70 percent / AlCl3 / CH2Cl2 / 2 h / Ambient temperature View Scheme
参考文献
Wurm, Gotthard; Goessler, Bernd
Archiv der Pharmazie (Weinheim, Germany), 1989 , vol. 322, p. 569 - 572
反应条件
aluminium trichloride; sodium chloride T=200 - 220°C;
参考文献
Macbeth; Price; Winzor
Journal of the Chemical Society, 1935 , p. 325,327
Full Text Show Details
Kuroda; Wada
Scientific Papers of the Institute of Physical and Chemical Research (Japan), 1938 , vol. 34, p. 1740,1756,1758
Chem. Zentralbl., 1939 , vol. 110, # I p. 2792
参考文献
Nakata et al.
Tetrahedron Letters, 1959 , # 16 p. 9,13
