4-氯-2,3,5,6-四氟苯甲酰氯合成路线 （共 6 条）
反应条件
water; iron(III) chloride T=110 - 115°C; 1 h;
参考文献
Russian Journal of Organic Chemistry, , vol. 39, # 7 p. 975 - 978
反应条件
thionyl chloride; N,N-dimethyl-formamide 6 h; Heating; Yield given;
参考文献
Journal of Fluorine Chemistry, , vol. 59, # 1 p. 15 - 31
反应条件
1: aq. NaOH, NaHS / 2 h / 70 °C 2: 978 mg / 30percent H2O2, AcOH / 2 h / 70 °C 3: SOCl2, DMF / 6 h / Heating View Scheme
参考文献
Journal of Fluorine Chemistry, , vol. 59, # 1 p. 15 - 31
反应条件
1: 978 mg / 30percent H2O2, AcOH / 2 h / 70 °C 2: SOCl2, DMF / 6 h / Heating View Scheme
参考文献
Journal of Fluorine Chemistry, , vol. 59, # 1 p. 15 - 31
反应条件
water; iron(III) chloride T=110 - 115°C; 1 h; Product distribution; Further Variations:Temperaturesamounts of reactants;
参考文献
Russian Journal of Organic Chemistry, , vol. 39, # 7 p. 975 - 978
反应条件
1: NaF, Ph4PBr / various solvent(s) / 10 h / 155 °C
2: diethyl ether
View Scheme
参考文献
Fielding, H. C.; Shirley, I. M.
Journal of Fluorine Chemistry, 1992 , vol. 59, # 1 p. 15 - 31
