2,5-二苯基-1,3,4-噻二唑合成路线 （共 67 条）
反应条件
tert-butylhypochlorite in dichloromethane
T=-70 - -55°C; 0.333333 h;
参考文献
Demchuk, D. V.; Lutsenko, A. I.; Troyanskii, E. I.; Nikishin, G. I.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1989 , vol. 38, # 8.2 p. 1690 - 1695
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1989 , # 8 p. 1843 - 1848
反应条件
dihydrogen peroxide in ethanol
0.0166667 h; Heating;
参考文献
Kurzer, Frederick; Doyle, Kevin M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 1873 - 1880
反应条件
triethylamine in ethanol
24 h; Heating;
参考文献
Moss, Stephen F.; Taylor, David R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , # 9 p. 1999 - 2006
反应条件
1: 76 percent / 1.) 76percent NaOH, 2.) AcOH / 1.) H2O, room temp., 10 min, 2.) 0 deg C
2: 50 percent / pyridine / 4 h
View Scheme
参考文献
Kurzer, Frederic; Secker, Jane L.
Tetrahedron, 1981 , vol. 37, p. 1429 - 1436
反应条件
aluminum oxide; tetraphosphorus decasulfide
T=120°C; 0.166667 h; microwave irradiation;
参考文献
Polshettiwar, Vivek; Varma, Rajender S.
Tetrahedron Letters, 2008 , vol. 49, # 5 p. 879 - 883
反应条件
sulfur in benzene
14 h; Heating;
参考文献
Aly, Moustafa F.; Grigg, Ronald
Tetrahedron, 1988 , vol. 44, # 23 p. 7271 - 7282
反应条件
sodium hydroxide in water
Ambient temperature;
参考文献
Kurzer, Frederic; Secker, Jane L.
Tetrahedron, 1981 , vol. 37, p. 1429 - 1436
反应条件
pyridine in methanol
Heating;
参考文献
Poddubnyi; Belen'kii; Krayushkin
Russian Chemical Bulletin, 1996 , vol. 45, # 5 p. 1185 - 1188
反应条件
dithiophosphoric acid O,O-diethyl ester
T=100°C; 12 h;
参考文献
Pudovik, A. N.; Khairullin, V. K.; Pudovik, M. A.; Musin, R. Z.
Russian Journal of General Chemistry, 1995 , vol. 65, # 1.2 p. 140 - 141
Zhurnal Obshchei Khimii, 1995 , vol. 65, # 1 p. 158 - 159
反应条件
tert-butylhypochlorite in dichloromethane
T=-70 - -55°C; 0.333333 h;
参考文献
Demchuk, D. V.; Lutsenko, A. I.; Troyanskii, E. I.; Nikishin, G. I.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1989 , vol. 38, # 8.2 p. 1690 - 1695
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1989 , # 8 p. 1843 - 1848
