3-苯基-2-硫酮-1,3-噻唑啉-4-酮合成路线 (共 53 条)
反应条件
in water 3 h; Reflux;
参考文献
The Johns Hopkins University; Southern Methodist University; Biehl, Edward R.; Kamila, Sukanta; Dawson, Ted M.
Patent: US2013/253021 A1, 2013 ;
Location in patent: Paragraph 0055; 0056 ;
反应条件
potassium carbonate; aniline in water
参考文献
Cell Therapeutics, Inc.
Patent: US2004/2526 A1, 2004 ;
反应条件
1: carbon disulfide; aniline With sodium hydroxide in water T=100°C; Microwave irradiation; 2: chloroacetic acid in water T=100°C; 0.0833333 h; Microwave irradiation; 3: With hydrogenchloride in water T=120°C; 0.5 h; Microwave irradiation;
参考文献
Nitsche, Christoph; Klein, Christian D.
Tetrahedron Letters, 2012 , vol. 53, # 39 p. 5197 - 5201
参考文献
Seyfried; Linden; Mloston; Heimgartner
Polish Journal of Chemistry, 2006 , vol. 80, # 8 p. 1363 - 1376
反应条件
triethylamine in dichloromethane T=20°C;
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 15, # 14 p. 3374 - 3379
反应条件
1: KOH / diethyl ether; ethanol 2: aq. HCl / 0.25 h / Heating View Scheme
参考文献
Russian Journal of Organic Chemistry, , vol. 32, # 1 p. 133 - 134
反应条件
triethylamine in water; acetone 0.5 h;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 24, # 10 p. 1824 - 1825
Zhurnal Organicheskoi Khimii, , vol. 24, # 10 p. 2024 - 2026
反应条件
2-amino-benzenethiol in benzene 0.0833333 h; Heatingalso from 2-amino-5-methylbenzenethiol; or with triethylamine, pyridine or sodium carbonate; Yields of byproduct given;
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 23, # 5 p. 469 - 470
反应条件
triethylamine in benzene or with pyridine or sodium carbonate;
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 23, # 5 p. 469 - 470
参考文献
Monatshefte fuer Chemie, , vol. 25, p. 178