1-[(3S)-3-羟基-1-环己烯-1-基]乙酮合成路线 (共 1 条)
反应条件
1: imidazole / dimethylformamide / Ambient temperature 2: DIBAL-H / toluene / 0.17 h / -60 °C 3: 4-dimethylaminopyridine / CH2Cl2 / 0 - 20 °C 4: tributyltin hydride / 7 h / 160 °C 5: n-Bu4NF / tetrahydrofuran / Ambient temperature View Scheme
参考文献
Satoh, Tsuyoshi; Motohashi, Shigeyasu; Tokutake, Norio; Yamakawa, Koji
Bulletin of the Chemical Society of Japan, 1992 , vol. 65, # 11 p. 2966 - 2973