反应条件
1.1: sodium / ethanol / 20 h / 100 °C / |Sealed tube; |Darkness
2.1: copper(l) iodide; potassium carbonate; N,N-dimethylethylenediamine / toluene / 40 h / 110 °C / |Schlenk technique; |Inert atmosphere
2.2: 1 h / 90 °C
View Scheme
参考文献
Zhan, Fuxu; Liang, Guangxin
Angewandte Chemie - International Edition, 2013 , vol. 52, # 4 p. 1266 - 1269
Angew. Chem., 2012 , vol. 125, # 4 p. 1304 - 1307,4
