2-萘基-2,3,4,6-O-四乙酰基-β-吡喃葡萄糖苷合成路线 (共 8 条)
反应条件
Ag(1+)*C22H24AgN4(1+)*2Cl(1-) in acetonitrile T=25°C; 3 h; Darkness; stereoselective reaction;
参考文献
Talisman, Ian J.; Kumar, Vineet; Deschamps, Jeffrey R.; Frisch, Mark; Malhotra, Sanjay V.
Carbohydrate Research, 2011 , vol. 346, # 15 p. 2337 - 2341
反应条件
(benzyl)-tri-(butyl)-ammonium chloride; potassium carbonate in chloroform T=20°C; glycosylation;
参考文献
Hongu, Mitsuya; Saito, Kunio; Tsujihara, Kenji
Synthetic Communications, 1999 , vol. 29, # 16 p. 2775 - 2781
反应条件
4 A molecular sieve; boron trifluoride diethyl etherate in dichloromethane 48 h; Ambient temperature;
参考文献
Smits; Engberts; Kelogg; Van Doren
Molecular Crystals and Liquid Crystals Science and Technology Section A: Molecular Crystals and Liquid Crystals, 1995 , vol. 260, # pt 1 p. 185 - 199
反应条件
3 A molecular sieve in dichloromethane Ambient temperature;
参考文献
Danieli, Bruno; Peri, Francesco; Roda, Gabriella; Carrea, Giacomo; Riva, Sergio
Tetrahedron, 1999 , vol. 55, # 7 p. 2045 - 2060
反应条件
trimethylsilyl trifluoromethanesulfonate in dichloromethane T=20°C; 24 h; Yield given. Yields of byproduct given;
参考文献
Tetrahedron Letters, , vol. 23, # 45 p. 4661 - 4664
参考文献
Archiv der Pharmazie (Weinheim, Germany), , vol. 287, p. 38,44
反应条件
pyridine; acetic anhydride 1.) CH2Cl2, reflux, 4 h, 2.) room temperature, 24 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Carbohydrate Research, , vol. 285, p. 159 - 165
参考文献
Jermyn
Australian Journal of Chemistry, 1955 , vol. 8, p. 403,407
Australian Journal of Chemistry, 1954 , vol. 7, p. 202,204