5,7-二羟基-3,3,4,5-四甲氧基黄酮合成路线 （共 3 条）
反应条件
1: With triethylamine Allan-Robinson condensation; 0.0833333 h; Heating; 2: With potassium hydroxide in methanol 0.333333 h; sonication;
参考文献
Daskiewicz, Jean-Baptiste; Depeint, Flore; Viornery, Lionel; Bayet, Christine; Comte-Sarrazin, Geraldine; Comte, Gilles; Gee, Jennifer M.; Johnson, Ian T.; Ndjoko, Karine; Hostettmann, Kurt; Barron, Denis
Journal of Medicinal Chemistry, 2005 , vol. 48, # 8 p. 2790 - 2804
反应条件
1.1: 90 percent / methanesulfonyl chloride; Et3N / tetrahydrofuran / 0 °C 2.1: Et3N / 0.08 h / Heating 2.2: 62 percent / KOH / methanol / 0.33 h / sonication View Scheme
参考文献
Daskiewicz, Jean-Baptiste; Depeint, Flore; Viornery, Lionel; Bayet, Christine; Comte-Sarrazin, Geraldine; Comte, Gilles; Gee, Jennifer M.; Johnson, Ian T.; Ndjoko, Karine; Hostettmann, Kurt; Barron, Denis
Journal of Medicinal Chemistry, 2005 , vol. 48, # 8 p. 2790 - 2804
反应条件
sodium 3,4,5-trimethoxybenzoate T=175°C; Kochen des Reaktionsprodukts mit waessrig-alkoholischer Kalilauge;
参考文献
Kalff; Robinson
Journal of the Chemical Society, 1925 , vol. 127, p. 182
