反应条件
1: diisobutylaluminium hydride / hexane; dichloromethane / 2 h / 0 °C
2: tetra-(n-butyl)ammonium iodide; sodium hydride / N,N-dimethyl-formamide; mineral oil / 20 °C / Inert atmosphere
3: water; 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane; tert-butyl alcohol / 3 h / 0 - 20 °C / pH 7 / aq. phosphate buffer
View Scheme
参考文献
Alberch, Laura; Cheng, Gang; Seo, Seung-Kee; Li, Xuehua; Boulineau, Fabien P.; Wei, Alexander
Journal of Organic Chemistry, 2011 , vol. 76, # 8 p. 2532 - 2547
