3,5-二甲氧基-4-苯甲氧基安息香酸盐合成路线 （共 18 条）
反应条件
1: With potassium carbonate in N,N-dimethyl-formamide T=60°C; 20 h; Inert atmosphere; 2: With water; sodium hydroxide in methanol 1 h; Heating; 3: With hydrogenchloride in water
参考文献
Garcia, Gonzalo; Rodriguez-Puyol, Manuel; Alajarin, Ramon; Serrano, Isabel; Sanchez-Alonso, Patricia; Griera, Mercedes; Vaquero, Juan J.; Rodriguez-Puyol, Diego; Alvarez-Builla, Julio; Diez-Marques, Maria L.
Journal of Medicinal Chemistry, 2009 , vol. 52, # 22 p. 7220 - 7227
反应条件
water; sodium hydroxide in methanol 5 h; Reflux;
参考文献
Saez-Ayala, Magali; Fernandez-Perez, Maria Piedad; Chazarra, Soledad; McHedlishvili, Nani; Tarraga-Tomas, Alberto; Rodriguez-Lopez, Jose Neptuno
Molecules, 2013 , vol. 18, # 7 p. 8319 - 8341
反应条件
potassium carbonate in hexadeuterioacetone; water
参考文献
EP2730571 A1, ;
Page/Page column ;
反应条件
sodium hydroxide in methanol 9 h; Heating;
参考文献
Battersby, Alan R.; Jones, Raymond C. F.; Kazlauskas, Rymantas; Thornber, Craig W.; Ruchirawat, Somsak; Staunton, James
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 2016 - 2029
反应条件
sodium hydroxide durch Verseifung;
参考文献
Journal of the Chemical Society, , p. 1551
反应条件
1: K2CO3 / dimethylformamide 2: aq. KOH View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 51, # 9 p. 1085 - 1088
反应条件
1: TsOH / toluene 2: K2CO3 / dimethylformamide 3: aq. KOH View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 51, # 9 p. 1085 - 1088
反应条件
1: Bu4NHSO4, K2CO3 / toluene / 6 h / Heating 2: 2M aq. NaOH / various solvent(s) / 0.25 h View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 38, # 12 p. 2130 - 2137
反应条件
1: methanolic KOH-solution 2: NaOH-solution / durch Verseifung View Scheme
参考文献
Journal of the Chemical Society, , p. 1551
反应条件
1: sulfuric acid / 40 - 50 °C 2: NaOH-solution View Scheme
参考文献
Journal of the Chemical Society, , p. 1551
