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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
1459-62-7
合成路线
（共 9 条）
502-49-8
环辛酮
+
119-26-6
2,4-二硝基苯肼
→
反应条件
1459-62-7
反应条件
暂无反应条件数据
参考文献
Yusubov, Mekhman S.; Svitich, Dmitrii Yu.; Yoshimura, Akira; Nemykin, Victor N.; Zhdankin, Viktor V.
Chemical Communications, 2013 , vol. 49, # 96 p. 11269 - 11271
17696-11-6
8-溴辛酸
→
反应条件
1459-62-7
反应条件
1: SOCl2 / 3 h / Heating 2: 94.6 percent / Et3N / diethyl ether / 0.5 h / Ambient temperature 3: 78 percent / NaBH4, NaH, 2-propanol / dioxane / 1.) 70 deg C, 2.) reflux, 1 h 4: 98.4 percent / m-chloroperbenzoic acid / CH2Cl2 / Ambient temperature 5: tert-BuOK / dimethylsulfoxide; tetrahydrofuran / 0.17 h / Ambient temperature 6: Al-Hg / tetrahydrofuran; H2O / 0.67 h / Heating 7: conc. H2SO4 / ethanol / 0.33 h / Heating View Scheme
参考文献
Ohtsuka, Yasuo; Oishi, Takeshi
Chemical & Pharmaceutical Bulletin, 1983 , vol. 31, # 2 p. 454 - 465
73674-32-5
→
反应条件
1459-62-7
反应条件
1: Al-Hg / tetrahydrofuran; H2O / 0.67 h / Heating 2: conc. H2SO4 / ethanol / 0.33 h / Heating View Scheme
参考文献
Ohtsuka, Yasuo; Oishi, Takeshi
Chemical & Pharmaceutical Bulletin, 1983 , vol. 31, # 2 p. 454 - 465
73674-09-6
8-溴辛酰氯
→
反应条件
1459-62-7
反应条件
1: 94.6 percent / Et3N / diethyl ether / 0.5 h / Ambient temperature 2: 78 percent / NaBH4, NaH, 2-propanol / dioxane / 1.) 70 deg C, 2.) reflux, 1 h 3: 98.4 percent / m-chloroperbenzoic acid / CH2Cl2 / Ambient temperature 4: tert-BuOK / dimethylsulfoxide; tetrahydrofuran / 0.17 h / Ambient temperature 5: Al-Hg / tetrahydrofuran; H2O / 0.67 h / Heating 6: conc. H2SO4 / ethanol / 0.33 h / Heating View Scheme
参考文献
Ohtsuka, Yasuo; Oishi, Takeshi
Chemical & Pharmaceutical Bulletin, 1983 , vol. 31, # 2 p. 454 - 465
78082-10-7
→
反应条件
1459-62-7
反应条件
1: 78 percent / NaBH4, NaH, 2-propanol / dioxane / 1.) 70 deg C, 2.) reflux, 1 h 2: 98.4 percent / m-chloroperbenzoic acid / CH2Cl2 / Ambient temperature 3: tert-BuOK / dimethylsulfoxide; tetrahydrofuran / 0.17 h / Ambient temperature 4: Al-Hg / tetrahydrofuran; H2O / 0.67 h / Heating 5: conc. H2SO4 / ethanol / 0.33 h / Heating View Scheme
参考文献
Ohtsuka, Yasuo; Oishi, Takeshi
Chemical & Pharmaceutical Bulletin, 1983 , vol. 31, # 2 p. 454 - 465
73674-12-1
→
反应条件
1459-62-7
反应条件
1: 98.4 percent / m-chloroperbenzoic acid / CH2Cl2 / Ambient temperature 2: tert-BuOK / dimethylsulfoxide; tetrahydrofuran / 0.17 h / Ambient temperature 3: Al-Hg / tetrahydrofuran; H2O / 0.67 h / Heating 4: conc. H2SO4 / ethanol / 0.33 h / Heating View Scheme
参考文献
Ohtsuka, Yasuo; Oishi, Takeshi
Chemical & Pharmaceutical Bulletin, 1983 , vol. 31, # 2 p. 454 - 465
73674-22-3
→
反应条件
1459-62-7
反应条件
1: tert-BuOK / dimethylsulfoxide; tetrahydrofuran / 0.17 h / Ambient temperature 2: Al-Hg / tetrahydrofuran; H2O / 0.67 h / Heating 3: conc. H2SO4 / ethanol / 0.33 h / Heating View Scheme
参考文献
Ohtsuka, Yasuo; Oishi, Takeshi
Chemical & Pharmaceutical Bulletin, 1983 , vol. 31, # 2 p. 454 - 465
696-71-9
环辛醇
→
反应条件
1459-62-7
反应条件
1: 1-tosyloxy-1-oxo-1H-1λ5-benzo[d][1,2]iodoxol-3-one / dichloromethane / 0.17 h / 20 °C 2: sulfuric acid / water; ethanol View Scheme
参考文献
Yusubov, Mekhman S.; Svitich, Dmitrii Yu.; Yoshimura, Akira; Nemykin, Victor N.; Zhdankin, Viktor V.
Chemical Communications, 2013 , vol. 49, # 96 p. 11269 - 11271
97-00-7
1-氯-2,4-二硝基苯
→
反应条件
1459-62-7
反应条件
1: aq.-ethanolic ammonia; hydrazine hydrate View Scheme
参考文献
Brady
Journal of the Chemical Society, 1931 , p. 756,758
