1,3-金刚烷二羧酸二甲酯合成路线 (共 10 条)
反应条件
thionyl chloride; triethylamine in methanol; N,N-dimethyl-formamide
参考文献
Daicel Chemical Industries, Ltd.; Ishii, Yasutaka
Patent: EP897747 A1, 1999 ;
反应条件
sulfuric acid in water; 1,2-dichloro-ethane T=62°C; 10 h; Product distribution / selectivity;
参考文献
US7078562 B2, ;
Page/Page column 16-17; 19-20 ;
反应条件
1: 1-bromoadamantane; carbon monoxide With aluminum tri-bromide; carbon tetrabromide in methylene dibromide T=0 - 20°C; P=760.051 Torr; 3 h; 2: methanol in methylene dibromide T=0°C;
参考文献
Akhrem, Irena S.; Avetisyan, Dzhul'Etta V.; Afanas'Eva, Lyudmila V.; Goryunov, Evgenii I.; Churilova, Irina M.; Petrovskii, Pavel V.; Kagramanov, Nikolai D.
Mendeleev Communications, 2011 , vol. 21, # 5 p. 259 - 261
参考文献
Chemische Berichte, , vol. 74, p. 1769,1771
反应条件
1: Br2, BBr3 2: H2SO4, Ag2SO4 View Scheme
参考文献
Chemische Berichte, , vol. 93, p. 1366 - 1371
反应条件
1: H2SO4, Ag2SO4 View Scheme
参考文献
Chemische Berichte, , vol. 93, p. 1366 - 1371
参考文献
Chemische Berichte, , vol. 93, p. 1366 - 1371
反应条件
in diethyl ether Ambient temperature;
参考文献
Heagy, Michael D.; Wang, Qi; Olah, George A.; Prakash, G. K. Surya
Journal of Organic Chemistry, 1995 , vol. 60, # 22 p. 7351 - 7354
参考文献
Landa; Kamycek
Collection of Czechoslovak Chemical Communications, 1959 , vol. 24, p. 1320,1323
反应条件
lithium aluminium tetrahydride in tetrahydrofuran 70 h; Heating;
参考文献
Klaic, Lada; Aleskovic, Marija; Veljkovic, Jelena; Mlinaric-Majerski, Kata
Journal of Physical Organic Chemistry, 2008 , vol. 21, # 4 p. 299 - 305