tetrabutyl ammonium fluoride in tetrahydrofuran 0.5 h;
参考文献
Jeong, Lak S.; Shinazi, Raymond F.; Beach, J. Warren; Kim, Hea O.; Nampalli, Satyanarayana; et al.
Journal of Medicinal Chemistry, 1993 , vol. 36, # 2 p. 181 - 195
1: (NH4)2SO4 / 1 h / Heating 2: 60 percent / trimethylsilyl triflate (TMSOTf) / CH2Cl2 / 16 h / -20 - 20 °C 3: 23.4 percent / NH3(gas) / 1,2-dimethoxy-ethane / Ambient temperature 4: 74.7 percent / n-Bu4NF / tetrahydrofuran / 0.5 h View Scheme
参考文献
Jeong, Lak S.; Shinazi, Raymond F.; Beach, J. Warren; Kim, Hea O.; Nampalli, Satyanarayana; et al.
Journal of Medicinal Chemistry, 1993 , vol. 36, # 2 p. 181 - 195
1: 60 percent / trimethylsilyl triflate (TMSOTf) / CH2Cl2 / 16 h / -20 - 20 °C 2: 23.4 percent / NH3(gas) / 1,2-dimethoxy-ethane / Ambient temperature 3: 74.7 percent / n-Bu4NF / tetrahydrofuran / 0.5 h View Scheme
参考文献
Jeong, Lak S.; Shinazi, Raymond F.; Beach, J. Warren; Kim, Hea O.; Nampalli, Satyanarayana; et al.
Journal of Medicinal Chemistry, 1993 , vol. 36, # 2 p. 181 - 195
