1,3,5-三叔丁基苯合成路线 (共 102 条)
反应条件
aluminium trichloride T=0°C;
参考文献
Petroleum Chemistry, , vol. 47, # 6 p. 434 - 441
反应条件
methyl-magnesium iodide Behandeln des erhaltenen 2-<3,5-Di-tert-butyl-phenyl>-propan-2-ols mit Chlorwasserstoff und Behandeln des Reaktionsprodukts mit Methylmagnesiumjodid in Aether;
参考文献
Recueil des Travaux Chimiques des Pays-Bas, , vol. 75, p. 349,353
反应条件
magnesium T=500°C; flash vacuum pyrolysis; Mechanism;
参考文献
Tetrahedron Letters, , vol. 38, # 48 p. 8417 - 8420
反应条件
tert.-butyl lithium 1) THF, -78 deg C, 1 h; 2) THF, 60 deg C, 20 h; Multistep reaction;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 59, p. 2529 - 2536
反应条件
Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 59, p. 2529 - 2536
参考文献
Phosphorus and Sulfur and the Related Elements, , vol. 26, p. 83 - 90
反应条件
T=200°C; und Behandeln des Reaktionsgemisches mit verd.wss.Schwefelsaeure;
参考文献
Journal of the American Chemical Society, , vol. 76, p. 2349,2351
Journal of the American Chemical Society, , vol. 77, p. 2806,2811
反应条件
in tetrahydrofuran; diethyl ether byproducts: LiCl; addn. of soln. of HSiCl3 in THF to soln. of org.compd. in THF (-78°C), stirring (2 h, -78°C), addn. of (2)HCl in ether; distn., not sepd.; IR spectrometry;
参考文献
Zeitschrift fuer Anorganische und Allgemeine Chemie, , vol. 572, p. 186 - 191
反应条件
bromine in tetrachloromethane Ambient temperaturefurther solvent; other ratio of the reactants;; MechanismProduct distribution;
参考文献
Tetrahedron Letters, , vol. 25, # 4 p. 411 - 414
反应条件
in tetrahydrofuran T=-78°C; with quencher; Product distribution;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 60, # 3 p. 1037 - 1040