1,3,5-三叔丁基苯合成路线 （共 102 条）
反应条件
1: 67 percent / HNO3 / acetic anhydride; acetic acid / 50 h / Ambient temperature 2: 56 percent / 5percent sodium amalgam / methanol / 5 h / Heating View Scheme
参考文献
Bartlett et al.
Journal of the American Chemical Society, 1954 , vol. 76, p. 2349,2351
反应条件
aluminum tri-bromide T=-0.1 - 99.9°C; Equilibrium constantThermodynamic data;
参考文献
Russian Journal of Physical Chemistry, , vol. 58, # 2 p. 297 - 298
Zhurnal Fizicheskoi Khimii, , vol. 58, # 2 p. 491 - 493
反应条件
1: (bromination) 2: CuO, Cu, aq. NaOH / 275 °C View Scheme
参考文献
Canadian Journal of Chemistry, , vol. 41, # 7 p. 1653 - 1656
反应条件
1: AcOH, AgNO3, aq. HNO3, Br2 2: (i) nBuLi, (ii) I2 View Scheme
参考文献
Zimmermann,H.E.; Dodd,J.R.
Journal of the American Chemical Society, 1970 , vol. 92, # 22 p. 6507 - 6515
反应条件
1: (bromination) 2: CuO, Cu, aq. NaOH / 275 °C 3: aq. HNO3, AcOH / Ambient temperature View Scheme
参考文献
Elder,J.W.; Mariella,R.P.
Canadian Journal of Chemistry, 1963 , vol. 41, # 7 p. 1653 - 1656
反应条件
sulfuric acid in acetic acid T=20°C; Cooling with ice;
参考文献
Russian Journal of Organic Chemistry, , vol. 48, # 6 p. 780 - 782,3
反应条件
1: 70 percent / bromine, iron / CCl4 / 16 h / Ambient temperature 2: 71 percent / magnesium / tetrahydrofuran / 5 h / Heating View Scheme
参考文献
Komen, Corine M.D.; Bickelhaupt, Friedrich
Synthetic Communications, 1996 , vol. 26, # 9 p. 1693 - 1697
反应条件
aluminum tri-bromide T=-0.1 - 99.9°C; Equilibrium constantThermodynamic data;
参考文献
Nesterova, T. N.; Verevkin, S. P.; Karaseva, S. Ya.; Rozhnov, A. M.; Tsvetkov, V. F.
Russian Journal of Physical Chemistry, 1984 , vol. 58, # 2 p. 297 - 298
Zhurnal Fizicheskoi Khimii, 1984 , vol. 58, # 2 p. 491 - 493
反应条件
bromine; iron in tetrachloromethane T=20°C; 33 h;
参考文献
Nomura, Nobuyoshi; Ishii, Ryohei; Yamamoto, Yoshihiko; Kondo, Tadao
Chemistry - A European Journal, 2007 , vol. 13, # 16 p. 4433 - 4451
反应条件
bromine in tetrachloromethane
参考文献
BP Corporation North America Inc.
Patent: EP1157047 B1, 2003 ;
