N-BOC-N,2-二甲基丙氨酸合成路线 （共 3 条）
反应条件
sodium hydride in tetrahydrofuran T=0°C; 24 h;
参考文献
Guerlavais, Vincent; Boeglin, Damien; Mousseaux, Delphine; Oiry, Catherine; Heitz, Annie; Deghenghi, Romano; Locatelli, Vittorio; Torsello, Antonio; Ghe, Corrado; Catapano, Filomena; Muccioli, Giampiero; Galleyrand, Jean-Claude; Fehrentz, Jean-Alain; Martinez, Jean
Journal of Medicinal Chemistry, 2003 , vol. 46, # 7 p. 1191 - 1203
反应条件
tetreamethyl ammonium hydroxide in acetonitrile 72 h; Ambient temperature;
参考文献
Khalil, Ehab M.; Subasinghe, Nalin L.; Johnson, Rodney L.
Tetrahedron Letters, 1996 , vol. 37, # 20 p. 3441 - 3444
反应条件
1: 85 percent / DBU / acetonitrile / 0.5 h / 60 °C 2: 98 percent / 0.5 h / 0 °C 3: formic acid / H2O / 24 h / Heating 4: H2 / 10percent Pd/C / ethanol / 24 h View Scheme
参考文献
Guerlavais, Vincent; Boeglin, Damien; Mousseaux, Delphine; Oiry, Catherine; Heitz, Annie; Deghenghi, Romano; Locatelli, Vittorio; Torsello, Antonio; Ghe, Corrado; Catapano, Filomena; Muccioli, Giampiero; Galleyrand, Jean-Claude; Fehrentz, Jean-Alain; Martinez, Jean
Journal of Medicinal Chemistry, 2003 , vol. 46, # 7 p. 1191 - 1203
