N-(二乙基氨基甲酰)-N-甲氧甲酰胺合成路线 （共 8 条）
反应条件
1: 76 percent / Et3N / CHCl3 / 3 h / Heating 2: 1) AcCl, 2) 4-dimethylaminopyridine / 1) Et2O, 20 min, 2) CH2Cl2, 0 deg C, 2 h View Scheme
参考文献
Akikusa; Mitsui; Sakamoto; Kikugawa
Synthesis, 1992 , # 11 p. 1058 - 1060
反应条件
4-(N,N-dimethlyamino)pyridine; acetyl chloride 1) Et2O, 20 min, 2) CH2Cl2, 0 deg C, 2 h; Yield given. Multistep reaction;
参考文献
Akikusa; Mitsui; Sakamoto; Kikugawa
Synthesis, 1992 , # 11 p. 1058 - 1060
反应条件
sodium hydroxide in 1,4-dioxane T=60°C; 58 h;
参考文献
Akikusa; Mitsui; Sakamoto; Kikugawa
Synthesis, 1992 , # 11 p. 1058 - 1060
反应条件
in dichloromethane 4.5 h; Ambient temperature;
参考文献
Akikusa; Mitsui; Sakamoto; Kikugawa
Synthesis, 1992 , # 11 p. 1058 - 1060
反应条件
in dichloromethane 1 h; Ambient temperature;
参考文献
Akikusa; Mitsui; Sakamoto; Kikugawa
Synthesis, 1992 , # 11 p. 1058 - 1060
反应条件
T=60°C; 10.5 h; other primary amines and amino acids;
参考文献
Synthesis, , # 11 p. 1058 - 1060
反应条件
in dichloromethane 13 h; Ambient temperature;
参考文献
Akikusa; Mitsui; Sakamoto; Kikugawa
Synthesis, 1992 , # 11 p. 1058 - 1060
反应条件
sodium hydroxide in 1,4-dioxane 2 h; Ambient temperature;
参考文献
Akikusa; Mitsui; Sakamoto; Kikugawa
Synthesis, 1992 , # 11 p. 1058 - 1060
