反应条件
in acetone dropwise addn. of soln. of HgCl2 (62.2mmol) in acetone (40ml) to (C4H9)3SnCH2SC6H5 (62.3mmol) in acetone (50ml), -20°C, stirring; slow warming up at room temp.; stirring, 1h;; filtration of formed ppt., washing with acetone, recrystn. from hot acetone; yield of raw product: 92percent; elem. anal.;;
参考文献
Steinborn, Dirk; Sedlak, Ursula
Zeitschrift fuer Chemie (Stuttgart, Germany), 1985 , vol. 25, p. 376 - 377