反应条件
in neat (no solvent) GeCl3 was introduced into a N2-filled flask, Sn-compound was slowly added at room temp., the mixt. was stirred for 30 min at 50°C; selective condensation in a trap cooled at -30°C, kept in a freezer (-20°C);
参考文献
Strenalyuk, Tatyana; Samdal, Svein; Mollendal, Harald; Guillemin, Jean-Claude
Journal of Molecular Structure, 2006 , vol. 780-781, # SPEC. ISS. p. 157 - 162
