azobis(isobutyronitrile) in neat (no solvent) High Pressure; (Ar); addn. of AIBN to stannane, addn. of GeCl4, heating to 150°Cfor 5 h in a sealed tube, cooling to room temp.; dissolving in CH2Cl2, vac. distn.;
参考文献
Kultyshev, Roman G.; Prakash, G.K. Surya; Olah, George A.; Faller, Jack W.; Parr, Jonathan
Organometallics, 2004 , vol. 23, # 13 p. 3184 - 3188
α,α'-azobis(cyclohexylnitrile) in cyclohexane Kinetics; Irradiation (UV/VIS); reaction at 25°C in presence of α,α'-azobis(cyclohexylnitrile) and UV-irradiation;;
参考文献
Journal of the American Chemical Society, , vol. 90, p. 1055
hydrogenchloride in methanol; water Kinetics; byproducts: propene; excess HCl, 4percent water in MeOH, 18-29°C; not isolated, reaction followed by UV/VIS spectroscopy;
azobis(isobutyronitrile) in neat (no solvent) High Pressure; (Ar); addn. of AIBN to stannane, addn. of GeCl4, heating to 150°Cfor 33 h in a sealed tube, cooling to room temp.; dissolving in CH2Cl2, vac. distn.;
参考文献
Kultyshev, Roman G.; Prakash, G.K. Surya; Olah, George A.; Faller, Jack W.; Parr, Jonathan
Organometallics, 2004 , vol. 23, # 13 p. 3184 - 3188
azobis(isobutyronitrile) in neat (no solvent) High Pressure; (Ar); addn. of AIBN to stannane, addn. of GeCl4, heating to 150°Cfor 15 h in a sealed tube, cooling to room temp.; dissolving in CH2Cl2, vac. distn.;
参考文献
Kultyshev, Roman G.; Prakash, G.K. Surya; Olah, George A.; Faller, Jack W.; Parr, Jonathan
Organometallics, 2004 , vol. 23, # 13 p. 3184 - 3188
