catalyst: tetra-n-butylammonium iodide in neat (no solvent) byproducts: ethyl chloride; a mixt. of Bu3SnCl, EtI, and 5 molpercent of Bu4NI was heated slowly in an oil bath to 140°C over a period of 2.5 h, reaction was monitored byGLC; purifn. was accomplished by vac. distn. through a short path apparatus;
参考文献
Friedrich, Edwin C.; Abma, Charles B.; Delucca, George
Journal of Organometallic Chemistry, 1982 , vol. 228, # 3 p. 217 - 222