反应条件
in tetrahydrofuran addn. of vinyl bromide and ethylene dibromide to Mg in THF (N2 atmosphere), addn. of further vinyl bromide in THF during 1 h at reflux, decantation, addn. of Sn-compd., refluxing (1 h), cooling room temp.); evapn., partition (Et2O-H2O), washing etheral phase (H2O), drying, evapn., distn.; elem. anal.;
参考文献
Moloney, Mark G.; Pinhey, John T.; Stoermer, Martin J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry, 1990 , p. 2645 - 2656
