1: 2-methoxy-pyridine With n-butyllithium; 2-(dimethylamino)-ethanol in hexane T=-5 - 5°C; 1.5 h; 2: tributyltin chloride in hexane T=-78 - 20°C; 1 h; 3: With water in hexane T=0°C;
参考文献
PROLYSIS LTD.
Patent: WO2007/148093 A1, 2007 ;
Location in patent: Page/Page column 67 ;
WO 2007/148093 A1
1: 6-bromo-2-methoxypyridine With n-butyllithium in diethyl ether; hexane T=-78 - 0°C; 0.166667 h; 2: tributyltin chloride in diethyl ether; hexane T=-78 - 0°C; 1 h; 3: With water; ammonium chloride in diethyl ether; hexane
参考文献
DeGoey, David A.; Flentge, Charles A.; Flosi, William J.; Grampovnik, David J.; Kempf, Dale J.; Klein, Larry L.
Patent: US2005/131017 A1, 2005 ;
Location in patent: Page/Page column 148 ;
