trifluoroacetic acid; cobalt(II) dibromide; zinc in acetonitrile
CoBr2 and Zn dust activated with CF3CO2H reacted for 5 min with allyl chloride in MeCN, aryl halide and tributylstannyl chloride added simultaneously in MeCN at room temp., stirred for 1 h at 50°C;
参考文献
Gosmini, Corinne; Perichon, Jacques
Organic and Biomolecular Chemistry, 2005 , vol. 3, # 2 p. 216 - 217
trifluoroacetic acid; cobalt(II) dibromide; zinc in acetonitrile
CoBr2 and Zn dust activated with CF3CO2H reacted for 5 min with allyl chloride in MeCN, aryl halide and tributylstannyl chloride added simultaneously in MeCN at room temp., stirred for 2 h at 50°C;
参考文献
Gosmini, Corinne; Perichon, Jacques
Organic and Biomolecular Chemistry, 2005 , vol. 3, # 2 p. 216 - 217
trifluoroacetic acid; cobalt(II) dibromide; zinc in acetonitrile
CoBr2 and Zn dust activated with CF3CO2H reacted for 5 min with allyl chloride in MeCN, aryl halide and tributylstannyl chloride added simultaneously in MeCN at room temp., stirred for 4 h at 50°C;
参考文献
Gosmini, Corinne; Perichon, Jacques
Organic and Biomolecular Chemistry, 2005 , vol. 3, # 2 p. 216 - 217
in ethanol
byproducts: KCl; potassium bis(2-bromophenylamido)phosphate and Bu3SnCl heating for 30 min in refluxing EtOH, KCl removing, solvent evapg.; identified by elem. anal.;
参考文献
Lecat, J. L.; Devaud, M.
Polyhedron, 1983 , vol. 2, p. 1087 - 1090
