trans-[(2-tolyl)3P]2PdCl2 in xylene byproducts: o-Me-C6H4-CH2CN; mixt. of degassed educts heated at 120°C, until the color of mixt. turning to black (3 h); evapn., chromy. (silica gel), reduced pressure distn.;
trans-[(2-tolyl)3P]2PdCl2 in xylene byproducts: o-Cl-C6H4-CH2CN; mixt. of degassed educts heated at 120°C, until the color of mixt. turning to black (24 h); evapn., chromy. (silica gel), reduced pressure distn.;
