in diethyl ether to a stirred soln. of the ester (in dry ether) is added bromotrimethylsilane (in dry ether) dropwise; ether is removed at residual pressure of 7 Torr , fractionation;
参考文献
Journal of General Chemistry USSR (English Translation), , vol. 61, p. 837 - 840
Zhurnal Obshchei Khimii, , vol. 61, p. 921 - 925
in diethyl ether to a soln. of (CH3)3GeC((C4H9)3Sn)HCOOCH3 in dry ether is added with stirring (CH3)3GeBr; the reaction mixture is stirred for 96 h at room temp.; fractionation; elem. anal.;
参考文献
Nikolaeva, S. N.; Zolotareva, A. S.; Ponomarev, S. V.; Petrosyan, V. S.
Journal of General Chemistry USSR (English Translation), 1991 , vol. 61, p. 837 - 840
Zhurnal Obshchei Khimii, 1991 , vol. 61, p. 921 - 925
Delmond,B. et al.
Journal of Organometallic Chemistry, 1973 , vol. 47, p. 337 - 350
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Delmond et al.
Tetrahedron Letters, 1969 , p. 2089
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Gmelin Handbook: Sn: Org.Comp.12, 1.4.1.1.1.5.2.1.7, page 69 - 97
Delmond,B. et al.
Journal of Organometallic Chemistry, 1973 , vol. 47, p. 337 - 350
Full Text View citing articles Show Details
Delmond et al.
Tetrahedron Letters, 1969 , p. 2089
Full Text View citing articles Show Details
Gmelin Handbook: Sn: Org.Comp.12, 1.4.1.1.1.5.2.1.7, page 69 - 97
