反应条件
formic acid in not given byproducts: CO2, H2O; 100°C, stirring (4 h), then 200°C (200 Torr, 4 h), addn. of further formic acid, then 100°C (30 min); further product: Bu3SnOCHO; cooling to room temp., addn. of MeOH, decantation, addn. of petroleum ether, filtration, evapn., distn.; mixt. of products detd. by (119)Sn-NMRspectroscopy and liquid chromy.;
参考文献
Journal of Organometallic Chemistry, , vol. 294, p. C41 - C45
