反应条件
in tetrahydrofuran; n-heptane byproducts: C6H5S(O)2CH2Mg(s-Bu); under anaerobic conditions, in NMR tube; Sn compd., Mg compd. (molar ratio 1:1) in heptane, SnMe4 (internal standard) and THF mixed; reacted for1 h; not isolated; monitored by (119)Sn NMR spectra; > 95percent conversion;
参考文献
Journal of Organometallic Chemistry, , vol. 655, # 1-2 p. 111 - 114
