三(苄氧羰基)-L-精氨酸合成路线 （共 16 条）
反应条件
sodium hydroxide T=-10°C;
参考文献
Orlowska, Alicja; Drabarek, Stefania
Polish Journal of Chemistry, 1980 , vol. 54, # 10 p. 1893 - 1899
反应条件
1: (S)-N2-(benzyloxycarbonyl)-arginine With chloro-trimethyl-silane; N-ethyl-N,N-diisopropylamine 2: benzyl chloroformate
参考文献
Formanovsky; Popova; Mikhura
Russian Journal of Bioorganic Chemistry, 2009 , vol. 35, # 6 p. 752 - 758
反应条件
1: diisopropylethylamine (DiPEA) / 1,2-dichloro-ethane / 1.) RT, 30 min; 2.) 40-50 deg C 2: diisopropylethylamine (DiPEA) / 1,2-dichloro-ethane / Ambient temperature View Scheme
参考文献
Tetrahedron Letters, , vol. 39, # 20 p. 3349 - 3352
反应条件
bis(trimethyl-silyl)acetamide
参考文献
Orlowska, Alicja; Drabarek, Stefania
Polish Journal of Chemistry, 1980 , vol. 54, # 10 p. 1893 - 1899
反应条件
N-ethyl-N,N-diisopropylamine in 1,2-dichloro-ethane Yield given;
参考文献
Tetrahedron Letters, , vol. 32, # 42 p. 6025 - 6028
反应条件
N-ethyl-N,N-diisopropylamine in 1,2-dichloro-ethane Ambient temperature; Yield given;
参考文献
Tetrahedron Letters, , vol. 39, # 20 p. 3349 - 3352
反应条件
sodium hydroxide; benzyl chloroformate Reinigung ueber das Natrium-Salz;
参考文献
Journal of Organic Chemistry, , vol. 22, p. 1515,1518
Journal of the American Chemical Society, , vol. 81, p. 2878,2883
反应条件
1: triethylamine; chlorocarbonic acid isobutyl ester; CHCl3 / weiteres Reagens: Toluol; anschliessend Behandeln mit L-Valin-benzylester-toluol-4-sulfonat und Triaethylamin in CHCl3 2: palladium; methanol; acetic acid / Hydrogenation View Scheme
参考文献
Zervas et al.
Journal of the American Chemical Society, 1959 , vol. 81, p. 2878,2881
反应条件
1: triethylamine; chlorocarbonic acid isobutyl ester; CHCl3 / weiteres Reagens: Toluol; anschliessend Behandeln mit L-Asparaginsaeure-dibenzylester-toluol-4-sulfonat und Triaethylamin in CHCl3 2: palladium; methanol. acetic acid / Hydrogenation View Scheme
参考文献
Zervas et al.
Journal of the American Chemical Society, 1959 , vol. 81, p. 2878,2881
反应条件
1: ClCO2iBu 2: H2 / Pd View Scheme
参考文献
Weitzel; Eisele; Guglielmi; Stock; Renner
Hoppe-Seyler's Zeitschrift fuer physiologische Chemie, 1971 , vol. 352, # 12 p. 1735 - 1738
