叔-丁基 p-苯甲基氨基甲酸酯合成路线 （共 24 条）
反应条件
Yield given. Multistep reaction;
参考文献
Journal of Organic Chemistry, , vol. 56, # 26 p. 7288 - 7291
反应条件
trichlorosilane; triethylamine in benzene T=70°C; 24 h; other reagents: triethylamine/methyltrichlorosilane, triethylamine/dichlorodimethylsilane, triethylamine/chlorotrimethylsilane; Yield given;
参考文献
Chong, Pek Y.; Janicki, Slawomir Z.; Petillo, Peter A.
Journal of Organic Chemistry, 1998 , vol. 63, # 23 p. 8515 - 8521
反应条件
tert.-butylnitrite; 2-hydroxy-1,3-isoindolinedione; palladium diacetate in acetonitrile T=70°C; 24 h; Inert atmosphereSealed tube;
参考文献
Shu, Zhibin; Ye, Yuxuan; Deng, Yifan; Zhang, Yan; Wang, Jianbo
Angewandte Chemie - International Edition, 2013 , vol. 52, # 40 p. 10573 - 10576
Angew. Chem., 2013 , vol. 125, # 40 p. 10767 - 10770,4
反应条件
water T=100°C; 10 h; Inert atmosphere;
参考文献
Wang, Jia; Liang, Yan-Liang; Qu, Jin
Chemical Communications, 2009 , # 34 p. 5144 - 5146
反应条件
Cu(BF4)2
T=30 - 33°C; 0.166667 h;
参考文献
Chakraborti, Asit K.; Chankeshwara, Sunay V.
Organic and Biomolecular Chemistry, 2006 , vol. 4, # 14 p. 2769 - 2771
反应条件
1: N-(4-methylphenyl) allylcarbamate With thiophenol; [(pentamethylcyclopentadienyl)Ru(1,5-cyclooctadiene)Cl] in methanol; water
T=20°C;
2: di-tert-butyl dicarbonate With 4-(N,N-dimethlyamino)pyridine in methanol; water
T=0 - 20°C; 1 h; Further stages.;
参考文献
Streu, Craig; Meggers, Eric
Angewandte Chemie - International Edition, 2006 , vol. 45, # 34 p. 5645 - 5648
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; samarium diiodide in tetrahydrofuran
T=-78°C;
参考文献
Kim, Yong Hae; Park, Heui Sul
Synlett, 1998 , # 3 p. 261 - 262
反应条件
polymethylhydrosiloxane; palladium on activated charcoal in ethanol
T=20°C; 3 h;
参考文献
Chandrasekhar; Raji Reddy; Jagadeeshwar Rao
Synlett, 2001 , # 10 p. 1561 - 1562
反应条件
polymethylhydrosiloxane; palladium on activated charcoal in ethanol
T=20°C; 5 h;
参考文献
Chandrasekhar; Raji Reddy; Jagadeeshwar Rao
Synlett, 2001 , # 10 p. 1561 - 1562
反应条件
2-(di-tert-butylphosphino)-2'-isopropoxy-1,1'-binaphthyl; caesium carbonate; bis(dibenzylideneacetone)-palladium(0) in tert-butyl alcohol
T=100°C; 20 h; Inert atmosphere;
参考文献
Ma, Fangfang; Xie, Xiaomin; Zhang, Lei; Peng, Zhiyong; Ding, Lina; Fu, Lei; Zhang, Zhaoguo
Journal of Organic Chemistry, 2012 , vol. 77, # 12 p. 5279 - 5285
