叔-丁基 p-苯甲基氨基甲酸酯合成路线 （共 24 条）
反应条件
2-(di-tert-butylphosphino)-2'-isopropoxy-1,1'-binaphthyl; caesium carbonate; bis(dibenzylideneacetone)-palladium(0) in tert-butyl alcohol
T=100°C; 20 h; Inert atmosphere;
参考文献
Ma, Fangfang; Xie, Xiaomin; Zhang, Lei; Peng, Zhiyong; Ding, Lina; Fu, Lei; Zhang, Zhaoguo
Journal of Organic Chemistry, 2012 , vol. 77, # 12 p. 5279 - 5285
反应条件
copper(ll) bromide in tetrahydrofuran; hexane
T=50°C; Substitution; 0.0833333 h;
参考文献
Yamaguchi, Jun-ichi; Shusa, Yuji; Suyama, Takayuki
Tetrahedron Letters, 1999 , vol. 40, # 47 p. 8251 - 8254
反应条件
tin; ammonium chloride in methanol
T=25°C; 4.5 h; Sonication;
参考文献
Chandrasekhar; Narsihmulu; Jagadeshwar
Synlett, 2002 , # 5 p. 771 - 772
参考文献
Yale University
Patent: US6100398 A1, 2000 ;
反应条件
ammonium hydroxide; iron in methanol
T=25°C; Reduction; condensation; 1 h; sonication;
参考文献
Chandrasekhar; Narsihmulu
Tetrahedron Letters, 2000 , vol. 41, # 41 p. 7969 - 7972
反应条件
zinc(II) chloride in dichloromethane
T=20°C; 0.333333 h;
参考文献
Arifuddin, M.; Lakshmikant, N.; Rajasekar, N.; Shinde, D. B.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 2012 , vol. 51, # 8 p. 1168 - 1172,5
参考文献
Choppin; Rogers
Journal of the American Chemical Society, 1948 , vol. 70, p. 2967
反应条件
1: bis-[(trifluoroacetoxy)iodo]benzene / 1,2-dichloro-ethane / 0.03 h / |Molecular sieve; |Inert atmosphere
2: 1,2-dichloro-ethane / 1 h / 60 °C / |Molecular sieve; |Inert atmosphere
View Scheme
参考文献
Reddy, N. Veera; Prasad, K. Rajendra; Reddy, P. Sudhir; Lakshmi Kantam; Reddy, K. Rajender
Organic and Biomolecular Chemistry, 2014 , vol. 12, # 14 p. 2172 - 2175
反应条件
1: TolSO2N=IPh / dichloromethane / 0.5 h / 20 °C / Inert atmosphere
2: dichloromethane / 4.5 h / 20 °C / Inert atmosphere
View Scheme
参考文献
Yoshimura, Akira; Luedtke, Matthew W.; Zhdankin, Viktor V.
Journal of Organic Chemistry, 2012 , vol. 77, # 4 p. 2087 - 2091
参考文献
Stanley,R.L.; Tarbebell,D.S.
Journal of Organic Chemistry, 1977 , vol. 42, # 23 p. 3686 - 3690
