1: -196.1 °C / Irradiation
2: diethyl ether; various solvent(s) / 2 h / Irradiation
View Scheme
参考文献
Schmidt, Steven P.; Pinhas, Allan R.; Hammons, James H.; Berson, Jerome A.
Journal of the American Chemical Society, 1982 , vol. 104, # 24 p. 6822 - 6823
1: pyridine / 20 h / 0 °C
2: 75 percent / HgBr2, Mg / diethyl ether / 6 h
3: Bu3SnH, azobis<isobutyronitrile> (AIBN) / benzene / 1.5 h / Heating; also without solvent, at 75 deg C
View Scheme
参考文献
Apparu, Marcel; Crandall, Jack K.
Journal of Organic Chemistry, 1984 , vol. 49, # 12 p. 2125 - 2130
1: 94 percent / CuI / diethyl ether / 4 h / Ambient temperature
2: pyridine / 20 h / 0 °C
3: 75 percent / HgBr2, Mg / diethyl ether / 6 h
4: Bu3SnH, azobis<isobutyronitrile> (AIBN) / benzene / 1.5 h / Heating; also without solvent, at 75 deg C
View Scheme
参考文献
Apparu, Marcel; Crandall, Jack K.
Journal of Organic Chemistry, 1984 , vol. 49, # 12 p. 2125 - 2130
in diethyl ether
2 h; Irradiation; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Schmidt, Steven P.; Pinhas, Allan R.; Hammons, James H.; Berson, Jerome A.
Journal of the American Chemical Society, 1982 , vol. 104, # 24 p. 6822 - 6823
