1-溴-2-氯甲氧基-乙烷合成路线 (共 12 条)
反应条件
hydrogenchloride in dichloromethane; pentane T=0°C; 0.5 h;
参考文献
Stefan, Eric; Nalin, Ansel P.; Taylor, Richard E.
Tetrahedron, 2013 , vol. 69, # 36 p. 7706 - 7712
反应条件
hydrogenchloride Ambient temperature;
参考文献
Ogle, C. A.; Wilson, T. E.; Stowe, J. A.
Synthesis, 1990 , # 6 p. 495 - 496
反应条件
hydrogenchloride 1.) 0 deg C, 1 h; 2.) r.t., 2 h;
参考文献
Everett, Jeremy R.; Hatton, Ian K.; Hunt, Eric; Tyler, John W.; Williams, David J.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1989 , p. 1719 - 1728
参考文献
Cresson,P.
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1965 , vol. 261, p. 1707 - 1709
反应条件
ammonium sulfate; tetrabutyl ammonium fluoride 1.) hexamethyldisilazane, reflux, 24 h; 2.) THF/benzene, reflux, 3 h; Yield given. Multistep reaction;
参考文献
Hakimelahi; Khalafi-Nezhad
Helvetica Chimica Acta, 1989 , vol. 72, # 7 p. 1495 - 1500
反应条件
sodium; N,N-dimethyl-aniline in benzene
参考文献
Mamedov,S.; Agaev,A.S.
J. Gen. Chem. USSR (Engl. Transl.), 1963 , vol. 33, # 10 p. 3166 - 3171,3093 - 3098
参考文献
Cresson,P.
Bulletin de la Societe Chimique de France, 1964 , p. 2629 - 2635
参考文献
Ogle, C. A.; Wilson, T. E.; Stowe, J. A.
Synthesis, 1990 , # 6 p. 495 - 496
反应条件
potassium hydroxide
2.) acetone, room temp., 48 h; Yield given. Multistep reaction;
参考文献
Kim, Kyung Eun; Adolph, Horst G.
Synthesis, 1987 , # 11 p. 1029 - 1030
参考文献
Mamedov,S.; Agaev,A.S.
J. Gen. Chem. USSR (Engl. Transl.), 1963 , vol. 33, # 10 p. 3166 - 3171,3093 - 3098