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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
14621-04-6
合成路线
（共 36 条）
106-43-4
对氯甲苯
+
363-72-4
五氟苯
→
反应条件
14621-04-6
反应条件
dicyclohexyl(2′,6′-dimethoxybiphenyl-2-yl)phosphine; palladium diacetate; potassium carbonate in isopropanol acetate T=80°C; 12 h;
参考文献
Lafrance, Marc; Shore, Daniel; Fagnou, Keith
Organic Letters, 2006 , vol. 8, # 22 p. 5097 - 5100
106-38-7
对溴甲苯
+
363-72-4
五氟苯
→
反应条件
14621-04-6
反应条件
P(t-Bu)2Me*HBF4; potassium carbonate; palladium diacetate in N,N-dimethyl acetamide T=120°C;
参考文献
Lafrance, Marc; Rowley, Christopher N.; Woo, Tom K.; Fagnou, Keith
Journal of the American Chemical Society, 2006 , vol. 128, # 27 p. 8754 - 8756
363-72-4
五氟苯
→
反应条件
14621-04-6
反应条件
palladium diacetate; silver(l) oxide in 1-methyl-pyrrolidin-2-one T=100°C; 15 h; GloveboxSchlenk technique; Reagent/catalystSolvent;
参考文献
Fang, Xin; Huang, Yuanyuan; Chen, Xiaoqing; Lin, Xiaoxi; Bai, Zhengshuai; Huang, Kuo-Wei; Yuan, Yaofeng; Weng, Zhiqiang
Journal of Fluorine Chemistry, 2013 , vol. 151, p. 50 - 57
106-38-7
对溴甲苯
→
反应条件
14621-04-6
反应条件
palladium diacetate; potassium carbonate; silver(l) oxide; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in toluene T=100°C; 8 h; Inert atmosphere; Reagent/catalyst;
参考文献
Shabalin, Anton Yu.; Adonin, Nicolay Y.; Bardin, Vadim V.; Parmon, Valentin N.
Tetrahedron, 2014 , vol. 70, # 23 p. 3720 - 3725
624-31-7
4-碘甲苯
+
363-72-4
五氟苯
→
反应条件
14621-04-6
反应条件
P(t-Bu)2Me*HBF4; silver trifluoromethanesulfonate; potassium carbonate; palladium diacetate in N,N-dimethyl acetamide T=120°C;
参考文献
Lafrance, Marc; Rowley, Christopher N.; Woo, Tom K.; Fagnou, Keith
Journal of the American Chemical Society, 2006 , vol. 128, # 27 p. 8754 - 8756
363-72-4
五氟苯
+
459-44-9
4-甲基偶氮苯四氟硼酸盐
→
反应条件
14621-04-6
反应条件
potassium phosphate; copper(l) iodide; 1,10-phenanthroline; tetra-(n-butyl)ammonium iodide in dimethyl sulfoxide; acetonitrile T=130°C; 4 h; Inert atmosphereSchlenk technique;
参考文献
Zhu, Xingyi; Li, Feng; Su, Weike
Tetrahedron Letters, 2013 , vol. 54, # 10 p. 1285 - 1289
106-38-7
对溴甲苯
+
58521-27-0
→
反应条件
14621-04-6
反应条件
palladium diacetate; tris-(o-tolyl)phosphine in diethylene glycol dimethyl ether T=130°C; 24 h; Inert atmosphereSealed tube;
参考文献
Shang, Rui; Xu, Qing; Jiang, Yuan-Ye; Wang, Yan; Liu, Lei
Organic Letters, 2010 , vol. 12, # 5 p. 1000 - 1003
106-38-7
对溴甲苯
+
1582-24-7
五氟苯硼酸
→
反应条件
14621-04-6
反应条件
tri-tert-butyl phosphine; cesium fluoride; silver(l) oxide; tris-(dibenzylideneacetone)dipalladium(0) in N,N-dimethyl-formamide T=100°C; Suzuki-Miyaura coupling; 12 h;
参考文献
Korenaga, Toshinobu; Kosaki, Takahiro; Fukumura, Rokki; Ema, Tadashi; Sakai, Takashi
Organic Letters, 2005 , vol. 7, # 22 p. 4915 - 4917
624-31-7
4-碘甲苯
+
58521-27-0
→
反应条件
14621-04-6
反应条件
copper(l) iodide in diethylene glycol dimethyl ether T=130°C; 24 h; Inert atmosphere;
参考文献
Shang, Rui; Fu, Yao; Wang, Yan; Xu, Qing; Yu, Hai-Zhu; Liu, Lei
Angewandte Chemie - International Edition, 2009 , vol. 48, # 49 p. 9350 - 9354
106-38-7
对溴甲苯
→
反应条件
784-14-5
2,3,4,5,6-五氟联苯
+
363-72-4
五氟苯
+
14621-04-6
反应条件
palladium diacetate; potassium carbonate; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene; silver(l) oxide in toluene T=100°C; 8 h; Inert atmosphere; Reagent/catalyst;
参考文献
Shabalin, Anton Yu.; Adonin, Nicolay Y.; Bardin, Vadim V.; Parmon, Valentin N.
Tetrahedron, 2014 , vol. 70, # 23 p. 3720 - 3725
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