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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
14621-04-6
合成路线
（共 36 条）
363-72-4
五氟苯
+
824-79-3
对甲苯亚磺酸钠
→
反应条件
14621-04-6
反应条件
Na3PO4*12H2O; silver carbonate; palladium dichloride in water; dimethyl sulfoxide T=100°C; 18 h; Schlenk technique;
参考文献
Miao, Tao; Wang, Lei
Advanced Synthesis and Catalysis, 2014 , vol. 356, # 2-3 p. 429 - 436
106-38-7
对溴甲苯
+
363-72-4
五氟苯
+
402-43-7
对溴三氟甲苯
→
反应条件
14621-04-6
反应条件
potassium phosphate; 1,10-phenanthroline; copper(l) iodide in N,N-dimethyl-formamide T=125°C; 1 h; Product distribution / selectivity;
参考文献
THE UNIVERSITY OF HOUSTON SYSTEM
Patent: US2009/76266 A1, 2009 ;
Location in patent: Page/Page column 28 ;
624-31-7
4-碘甲苯
+
363-72-4
五氟苯
+
455-13-0
4-碘三氟甲苯
→
反应条件
14621-04-6
反应条件
potassium phosphate; 1,10-phenanthroline; copper(l) iodide in N,N-dimethyl-formamide T=125°C; 1 h; Product distribution / selectivity;
参考文献
THE UNIVERSITY OF HOUSTON SYSTEM
Patent: US2009/76266 A1, 2009 ;
Location in patent: Page/Page column 28 ;
363-72-4
五氟苯
+
18412-57-2
三乙氧基对苯甲基硅烷
→
反应条件
14621-04-6
反应条件
potassium fluoride; Ag2CO3; palladium diacetate in N,N-dimethyl acetamide T=120°C; 12 h; Inert atmosphereGloveboxSchlenk technique;
参考文献
Fan, Huixin; Shang, Yaping; Su, Weiping
European Journal of Organic Chemistry, 2014 , vol. 2014, # 16 p. 3323 - 3327
459-44-9
4-甲基偶氮苯四氟硼酸盐
→
反应条件
14621-04-6
反应条件
tetrakis(triphenylphosphine) palladium(0) in ethylene glycol dimethyl ether T=20°C;
参考文献
Frohn, Hermann-Josef; Adonin, Nicolay Yu.; Bardin, Vadim V.; Starichenko, Vladimir F.
Journal of Fluorine Chemistry, 2002 , vol. 117, # 2 p. 115 - 120
363-72-4
五氟苯
+
108-88-3
甲苯
→
反应条件
14621-04-6
+
890-02-8
反应条件
copper diacetate; palladium diacetate; sodium carbonate; 2,2,2-trimethylacetic acid in N,N-dimethyl acetamide T=110°C; 24 h; Inert atmosphere; regioselective reaction;
参考文献
Wei, Ye; Su, Weiping
Journal of the American Chemical Society, 2010 , vol. 132, # 46 p. 16377 - 16379
→
反应条件
363-72-4
五氟苯
+
14621-04-6
+
14547-85-4
反应条件
in tetrachloromethane 12 h; Irradiation;
参考文献
Chen, Qing-Yun; Li, Zhan-Ting
Journal of Organic Chemistry, 1993 , vol. 58, # 9 p. 2599 - 2604
108-88-3
甲苯
→
反应条件
363-72-4
五氟苯
+
14621-04-6
+
14547-85-4
反应条件
in tetrachloromethane 12 h; Irradiation;
参考文献
Chen, Qing-Yun; Li, Zhan-Ting
Journal of Organic Chemistry, 1993 , vol. 58, # 9 p. 2599 - 2604
106-44-5
对甲酚
→
反应条件
14621-04-6
反应条件
1: pyridine / dichloromethane / 0 - 20 °C / Inert atmosphere 2: potassium acetate; palladium diacetate; 2-(dicyclohexylphosphino)-2'-methylbiphenyl / tetrahydrofuran / 17 h / 25 °C / Inert atmosphere View Scheme
参考文献
Chang, Joyce Wei Wei; Chia, Eugene Yurong; Chai, Christina Li Lin; Seayad, Jayasree
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 11 p. 2289 - 2299
106-38-7
对溴甲苯
+
363-72-4
五氟苯
→
反应条件
784-14-5
2,3,4,5,6-五氟联苯
+
14621-04-6
反应条件
palladium diacetate; caesium carbonate; tri-cyclo-hexyl-phosphine in toluene T=80°C; 3 h; Inert atmosphereSchlenk technique; Reagent/catalystSolvent; Overall yield = 95 percent;
参考文献
Ma, Xiaowei; Liu, Yan; Liu, Ping; Xie, Jianwei; Dai, Bin; Liu, Zhiyong
Applied Organometallic Chemistry, 2014 , vol. 28, # 3 p. 180 - 185
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