二(三甲基甲硅烷基)乙炔合成路线 （共 218 条）
反应条件
tetrakis(triphenylphosphine) palladium(0); copper(l) chloride in N,N-dimethyl-formamide T=80°C; sila-Sonogashira reaction; 6 h;
参考文献
Nishihara, Yasushi; Inoue, Eiji; Noyori, Shintaro; Ogawa, Daisuke; Okada, Yoshiaki; Iwasaki, Masayuki; Takagi, Kentaro
Tetrahedron, 2012 , vol. 68, # 24 p. 4869 - 4881
反应条件
tetrakis(triphenylphosphine) palladium(0); copper(l) chloride in N,N-dimethyl-formamide T=80°C; cross-coupling; 12 h;
参考文献
Nishihara, Yasushi; Ikegashira, Kazutaka; Hirabayashi, Kazunori; Ando, Jun-Ichi; Mori, Atsunori; Hiyama, Tamejiro
Journal of Organic Chemistry, 2000 , vol. 65, # 6 p. 1780 - 1787
反应条件
2,3,4,5-tetrakis(carbomethoxy)-spiro-glyoxalbis(2,6-diisopropylphenylimine)palladacyclopenta-2,4-diene in toluene T=80°C; 22 h;
参考文献
Dieck, Heindirk tom; Munz, Christina; Mueller, Christiane
Journal of Organometallic Chemistry, 1990 , vol. 384, p. 243 - 255
反应条件
aluminium trichloride CH2Cl2, 1.) 15 min, 22 deg C, 2.) 12 h, 22 deg C; Yield given. Multistep reaction;
参考文献
Steglich, Wolfgang; Wegmann, Helmut
Synthesis, 1980 , # 6 p. 481 - 483
反应条件
1: AlCl3 / CH2Cl2 / 0 - 25 °C 2: 4.13 g / dimethylformamide / 20 h / 20 °C View Scheme
参考文献
Iso, Yasuyoshi; Grajkowska, Ewa; Wroblewski, Jarda T.; Davis, Jared; Goeders, Nicholas E.; Johnson, Kenneth M.; Sanker, Subramaniam; Roth, Bryan L.; Tueckmantel, Werner; Kozikowski, Alan P.
Journal of Medicinal Chemistry, 2006 , vol. 49, # 3 p. 1080 - 1100
反应条件
aluminium trichloride in dichloromethane 12 h; Ambient temperature;
参考文献
Eisch, John J.; Behrooz, Mohammad; Dua, Suresh K.
Journal of Organometallic Chemistry, 1985 , vol. 285, p. 121 - 136
反应条件
aluminium trichloride in dichloromethane
参考文献
Otten, Albert; Namyslo, Jan Christoph; Stoermer, Martin; Kaufmann, Dieter E.
European Journal of Organic Chemistry, 1998 , # 9 p. 1997 - 2001
反应条件
1: AlCl3 / CH2Cl2 / 0 - 25 °C 2: 9.40 g / dimethylformamide / 17 h / 25 °C View Scheme
参考文献
Cosford, Nicholas D. P.; Tehrani, Lida; Roppe, Jeffrey; Schweiger, Edwin; Smith, Nicholas D.; Anderson, Jeffrey; Bristow, Linda; Brodkin, Jesse; Jiang, Xiaohui; McDonald, Ian; Rao, Sara; Washburn, Mark; Varney, Mark A.
Journal of Medicinal Chemistry, 2003 , vol. 46, # 2 p. 204 - 206
反应条件
(Me2SiCp''2UBu)2O*2THF in tetrahydrofuran T=66°C; 4 h; Product distribution; Further Variations:reaction time;
参考文献
Journal of the American Chemical Society, , vol. 128, # 29 p. 9350 - 9351
反应条件
(Me2SiCp''2UBu)2O*2THF in tetrahydrofuran T=66°C; 23 h; Product distribution; Further Variations:reaction time;
参考文献
Journal of the American Chemical Society, , vol. 128, # 29 p. 9350 - 9351
