二(三甲基甲硅烷基)乙炔合成路线 (共 218 条)
反应条件
(i) nBuLi, Et2O, (ii) /BRN= 1209714/; Multistep reaction;
参考文献
Priester,W.; West,R.
Journal of the American Chemical Society, 1976 , vol. 98, p. 8421 - 8425
反应条件
aluminium trichloride in dichloromethane
T=-55°C; 1 h;
参考文献
Capozzi, Giuseppe; Ottana, Rosaria; Romeo, Giovanni; Marcuzzi, Franco
Gazzetta Chimica Italiana, 1985 , vol. 115, # 6 p. 311 - 314
反应条件
η5-cyclopentadienyl dicarbonyl cobalt in toluene
Heating;
参考文献
Funk,R.L.; Vollhardt,K.P.
Journal of the American Chemical Society, 1980 , vol. 102, p. 5245
反应条件
η5-cyclopentadienyl dicarbonyl cobalt in octane
Heating;
参考文献
Funk,R.L.; Vollhardt,K.P.
Journal of the American Chemical Society, 1980 , vol. 102, p. 5245
反应条件
η5-cyclopentadienyl dicarbonyl cobalt
117 h; Heating;
参考文献
Funk,R.L.; Vollhardt,K.P.
Journal of the American Chemical Society, 1980 , vol. 102, p. 5245
反应条件
η5-cyclopentadienyl dicarbonyl cobalt
Heating;
参考文献
Funk,R.L.; Vollhardt,K.P.
Journal of the American Chemical Society, 1980 , vol. 102, p. 5245
反应条件
η5-cyclopentadienyl dicarbonyl cobalt
Heating;
参考文献
Funk,R.L.; Vollhardt,K.P.
Journal of the American Chemical Society, 1980 , vol. 102, p. 5245
反应条件
1: 64 percent / 18 h / 70 °C
2: 55 percent / benzene / 18 h / 70 °C
View Scheme
参考文献
Seyferth, Dietmar; Annarelli, Dennis C.; Vick, Steven C.
Journal of Organometallic Chemistry, 1984 , vol. 272, # 2 p. 123 - 140
反应条件
1: 64 percent / 18 h / 70 °C
2: 55 percent / benzene / 18 h / 70 °C
View Scheme
参考文献
Seyferth, Dietmar; Annarelli, Dennis C.; Vick, Steven C.
Journal of Organometallic Chemistry, 1984 , vol. 272, # 2 p. 123 - 140
反应条件
1: 64 percent / 18 h / 70 °C
2: 2.) O2 / 1.) benzene, 70 deg C, 18 h, 2.) benzene, 30 min
View Scheme
参考文献
Seyferth, Dietmar; Annarelli, Dennis C.; Vick, Steven C.
Journal of Organometallic Chemistry, 1984 , vol. 272, # 2 p. 123 - 140