二(三甲基甲硅烷基)乙炔合成路线 （共 218 条）
反应条件
T=650°C; P=0.001 Torr; Further byproducts given;
参考文献
Chemistry Letters, , # 8 p. 1441 - 1444
参考文献
Ho, Mei Sing; Wong, Henry N. C.
Journal of the Chemical Society, Chemical Communications, 1989 , # 17 p. 1238 - 1240
参考文献
Journal of the American Chemical Society, , vol. 74, p. 4853,4855
Doklady Akademii Nauk SSSR, , vol. 86, p. 551
Chem.Abstr., , p. 12225
反应条件
T=400°C; P=0.001 Torr; 3 h; Yield given. Title compound not separated from byproducts;
参考文献
Hoffmann, Reinhard W.; Riemann, Achim; Mayer, Bernhard
Chemische Berichte, 1985 , vol. 118, # 6 p. 2493 - 2513
反应条件
thermolysis at 120°C; condensation into CD2Cl2 at -80°C, NMR;
参考文献
Pilz, Monika; Michel, Holger; Berndt, Arnim
Angewandte Chemie, 1990 , vol. 102, p. 438 - 439
反应条件
in benzene-d6 T=120°C; 2 h;
参考文献
Journal of the American Chemical Society, , vol. 133, # 30 p. 11504 - 11507
反应条件
1: methyllithium / tetrahydrofuran 2: toluene / 9 h / 20 °C 3: benzene-d6 / 2 h / 120 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 133, # 30 p. 11504 - 11507
反应条件
tert.-butyl lithium 1.) THF, pentan, from -78 to -25 deg C, 2.) -78 deg C, overnight; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Journal of Organic Chemistry, , vol. 50, # 25 p. 5410 - 5413
反应条件
1: 1.) reflux, 24 h, 2.) hexane, reflux 30 h 2: 20 percent / hexane / 1 h / Irradiation 3: 60 percent Chromat. / benzene / 15 h / Ambient temperature; Irradiation View Scheme
参考文献
Journal of Organometallic Chemistry, , vol. 194, # 2 p. 147 - 158
反应条件
1: 20 percent / hexane / 1 h / Irradiation 2: 60 percent Chromat. / benzene / 15 h / Ambient temperature; Irradiation View Scheme
参考文献
Journal of Organometallic Chemistry, , vol. 194, # 2 p. 147 - 158
