1-三甲基甲硅烷基-3,3-二甲基-1-丁炔合成路线 （共 28 条）
反应条件
iron(III) chloride in tetrachloromethane; toluene T=25°C; 144 h; Product distribution;
参考文献
Bulletin de la Societe Chimique de France, , vol. 2, # 1-2 p. 16 - 20
反应条件
18-crown-6 ether; cesium fluoride in benzene T=20°C; 5 h;
参考文献
Journal of Organometallic Chemistry, , vol. 634, # 1 p. 69 - 73
反应条件
1: carbon monoxide; tri-phenyl-antimony With [bis(acetoxy)iodo]benzene in dichloromethane T=20°C; 7 h; 2: 1-(tert-butyl)-2-(trimethylsilyl)acetylene With tris(dibenzylideneacetone)dipalladium(0) chloroform complex; copper(l) iodide in acetonitrile T=50°C; 5 h; Further stages.;
参考文献
Kang, Suk-Ku; Ryu, Hyung-Chul; Hong, Young-Taek
Journal of the Chemical Society. Perkin Transactions 1, 2001 , # 7 p. 736 - 739
反应条件
anhydrous iron chloride in nitromethane T=-15°C; 6 h; Inert atmosphereSeal tube;
参考文献
Gandeepan, Parthasarathy; Parthasarathy, Kanniyappan; Su, Tsu-Hui; Cheng, Chien-Hong
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 2-3 p. 457 - 468
反应条件
n-butyllithium in hexane
3 h; Ambient temperature;
参考文献
Braun, Jacques; Trung, Bui Khac
Bulletin de la Societe Chimique de France, 1983 , vol. 2, # 1-2 p. 16 - 20
反应条件
in tetrahydrofuran
T=-20°C;
参考文献
Mai, Khuong; Patil, Ghanshyam
Journal of Organic Chemistry, 1986 , vol. 51, # 18 p. 3545 - 3548
反应条件
zinc(II) chloride in 1,2-dichloro-ethane
T=150°C; 0.25 h; microwave irradiation;
参考文献
Yeager, Adam R.; Min, Geanna K.; Porco Jr., John A.; Schaus, Scott E.
Organic Letters, 2006 , vol. 8, # 22 p. 5065 - 5068
反应条件
in gas
T=400°C; P=0.03 Torr; 6 h; Further byproducts given. Title compound not separated from byproducts;
参考文献
Maier, Guenther; Born, Dieter; Bauer, Ines; Wolf, Reinhard; Boese, Roland; Cremer, Dieter
Chemische Berichte, 1994 , vol. 127, # 1 p. 173 - 190
反应条件
T=-263.2°C; Irradiation;
参考文献
Maier, Guenter; Reuter, Karl Arnold; Reisenauer, Hans Peter
Tetrahedron Letters, 1985 , vol. 26, # 15 p. 1845 - 1848
反应条件
(Me2SiCp''2UBu)2O*2THF in tetrahydrofuran
T=66°C; 45 h; Product distribution; Further Variations:reaction time;
参考文献
Wang, Jiaxi; Gurevich, Ylia; Botoshansky, Mark; Eisen, Moris S.
Journal of the American Chemical Society, 2006 , vol. 128, # 29 p. 9350 - 9351
