1-三甲基甲硅烷基-3,3-二甲基-1-丁炔合成路线 （共 28 条）
反应条件
in tetrahydrofuran
1.) -78 deg C; 2.) up to RT; Yields of byproduct given;
参考文献
Eisch, John J.; Behrooz, Mohammad; Dua, Suresh K.
Journal of Organometallic Chemistry, 1985 , vol. 285, p. 121 - 136
参考文献
Courtneidge, John L.; Davies, Alwyn G.; Lusztyk, Ewa; Lusztyk, Janusz
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1984 , # 1 p. 155 - 164
反应条件
aluminium trichloride
参考文献
Capozzi, Giuseppe; Ottana, Rosaria; Romeo, Giovanni; Marcuzzi, Franco
Gazzetta Chimica Italiana, 1985 , vol. 115, # 6 p. 311 - 314
反应条件
in gas
T=400°C; P=0.03 Torr; 6 h; also photolysis, flash-pyrolysis and CuCl-catalyzed thermolysis, other products; Product distribution;
参考文献
Maier, Guenther; Born, Dieter; Bauer, Ines; Wolf, Reinhard; Boese, Roland; Cremer, Dieter
Chemische Berichte, 1994 , vol. 127, # 1 p. 173 - 190
参考文献
Neugebauer, Wolfgang; Geiger, Gottfried A. P.; Kos, Alexander J.; Stezowski, John J.; Schleyer, Paul von Rague
Chemische Berichte, 1985 , vol. 118, # 4 p. 1504 - 1516
反应条件
aluminium trichloride in dichloromethane
T=0°C; 0 - 10 deg C to r.t., 1 h;
参考文献
Hanack, Michael; Hassdenteufel, Juergen R.
Chemische Berichte, 1982 , vol. 115, # 2 p. 764 - 771
反应条件
1: With cesium fluoride in dimethyl sulfoxide
T=20°C; 3 h; Schlenk technique;
2: With hydrogenchloride in water
T=0°C; pH=> 1;
参考文献
Yonemoto-Kobayashi, Misato; Inamoto, Kiyofumi; Tanaka, Yoshiyuki; Kondo, Yoshinori
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 23 p. 3773 - 3775
反应条件
iron(III) chloride in tetrachloromethane; toluene
T=25°C; 144 h; Product distribution;
参考文献
Braun, Jacques; Trung, Bui Khac
Bulletin de la Societe Chimique de France, 1983 , vol. 2, # 1-2 p. 16 - 20
