O-[(叔丁基)二甲基硅烷基]-N-[芴甲氧羰基]-L-丝氨酸合成路线 (共 5 条)
反应条件
1: 91 percent / imidazole / dimethylformamide / 20 h / 25 °C 2: Na2CO3 / dioxane; H2O View Scheme
参考文献
Fischer, Peter M.
Tetrahedron Letters, 1992 , vol. 33, # 49 p. 7605 - 7608
反应条件
1: N-methylimidazole / dimethylformamide / 18 h / Ambient temperature 2: 10percent aq. citric acid / H2O / pH 4 View Scheme
参考文献
Fischer, Peter M.
Tetrahedron Letters, 1992 , vol. 33, # 49 p. 7605 - 7608
反应条件
sodium carbonate in 1,4-dioxane; water
参考文献
Luo, Yue; Evindar, Ghotas; Fishlock, Dan; Lajoie, Gilles A
Tetrahedron Letters, 2001 , vol. 42, # 23 p. 3807 - 3809
反应条件
1H-imidazole in N,N-dimethyl-formamide
参考文献
Luo, Yue; Evindar, Ghotas; Fishlock, Dan; Lajoie, Gilles A
Tetrahedron Letters, 2001 , vol. 42, # 23 p. 3807 - 3809
反应条件
trifluoroacetic acid in dichloromethane T=22°C; 0.25 h; other protected amino acids, other concentration of trifluoroacetic acid, other temperatur, other reaction time, other deprotecting reagents;
参考文献
Tetrahedron Letters, , vol. 33, # 49 p. 7605 - 7608