sodium chloride in diethyl ether; water reaction mixture is poured into ice-cold satd. aq. NaCl soln.; ether layer is separated and evapd.; poured into dry xylene and cooled in ice-bath; ppt. impure compound;
参考文献
Cassaretto, F. P.; McLafferty, J. J.; Moore, C. E.
Analytica Chimica Acta, 1965 , vol. 32, p. 376 - 380
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Gmelin Handbook: B: B-Verb.8, 11.2.3, page 167 - 173
sodium chloride in tetrahydrofuran reaction mixture is stirred with Na2CO3, NaCl is added followed by extrn. with THF (or dimethoxymethane); solvent is evapd. in vac.;
参考文献
Holzapfel, H.; Richter, C.
J. Prakt. Chem. (4), 1964 , vol. 26, p. 15 - 23
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Gmelin Handbook: B: B-Verb.8, 11.2.3, page 167 - 173
tetrakis(triphenylphosphine) palladium(0); triethylamine in ethanol; water Suzuki coupling;
参考文献
Kuuloja, Noora M.; Kylmaelae, Tuula M.; Tois, Jan E.; Sjoeholm, Rainer E.; Franzen, Robert G.
Synthetic Communications, 2011 , vol. 41, # 7 p. 1052 - 1063
