2-溴甲基-6-吡啶甲酸甲酯合成路线 (共 4 条)
反应条件
N-bromosuccinmide; dibenzoyl peroxide in tetrachloromethane T=85°C; 72 h; Heating / reflux;
参考文献
Gillespie, Paul; Goodnow, Robert Alan; Tilley, Jefferson Wright
Patent: US2006/122256 A1, 2006 ;
Location in patent: Page/Page column 23 ;
US 20060122256 A1
反应条件
phosphorus tribromide in chloroform T=20°C; 4 h;
参考文献
Zeng, Xianshun; Coquiere, David; Alenda, Aurelie; Garrier, Eva; Prange, Thierry; Li, Yun; Reinaud, Olivia; Jabin, Ivan
Chemistry - A European Journal, 2006 , vol. 12, # 24 p. 6393 - 6402
反应条件
1: sodium tetrahydroborate / methanol / Cooling with ice 2: phosphorus tribromide / chloroform / 0 °C / Inert atmosphere View Scheme
参考文献
Journal of the American Chemical Society, , vol. 134, # 20 p. 8670 - 8683
反应条件
1: sulfuric acid / 22 h / Reflux 2: dibenzoyl peroxide; N-bromosuccinmide / tetrachloromethane / 21 h / Reflux View Scheme