1,2-双(二苯基膦)乙烷氯化镍合成路线 (共 19 条)
反应条件
1: not given 2: methanol; isopropyl alcohol View Scheme
参考文献
Ni: MVol.C2, 8.20, page 1073 - 1085
反应条件
1: water; ethanol 2: NaI / water; ethanol 3: not given 4: methanol; isopropyl alcohol View Scheme
参考文献
Ni: MVol.C2, 8.20, page 1073 - 1085
反应条件
in methanol; isopropyl alcohol in warm soln.; washing with ether, drying in vac.;
参考文献
Inorganic Chemistry, , vol. 5, p. 1968 - 1974
反应条件
1: not given 2: ethanol View Scheme
参考文献
Journal of the Chemical Society, , p. 3238 - 3241
反应条件
1: dichloromethane 2: NaI / water; ethanol 3: not given 4: ethanol View Scheme
参考文献
Journal of the Chemical Society, , p. 3238 - 3241
反应条件
1: not given 2: methanol; isopropyl alcohol View Scheme
参考文献
Ni: MVol.C2, 8.20, page 1073 - 1085
反应条件
2: not given 3: methanol; isopropyl alcohol View Scheme
参考文献
Ni: MVol.C2, 8.20, page 1073 - 1085
反应条件
in ethanol in warm soln.; diamagnetic form obtained from the filtrate of the paramagnetic form;
参考文献
Journal of the Chemical Society, , p. 3238 - 3241
Ni: MVol.C2, 8.20, page 1073 - 1085
反应条件
1: not given 2: ethanol View Scheme
参考文献
Journal of the Chemical Society, , p. 3238 - 3241
反应条件
in tetrahydrofuran under Ar, stirred for 2 h at 20°C; volume reduced, cooled to -78°C for 2 d, pptn. of (DPPE)2Ni, evapn. of mother liquor, recrystn. from toluene at -20°C, dried in vac. (20°C, 1 h); elem. anal.;
参考文献
Schaefer, H.; Binder, D.
Zeitschrift fuer Anorganische und Allgemeine Chemie, 1988 , vol. 557, p. 45 - 58