反应条件
1: tetrahydrofuran / 18 h / Ambient temperature 2: NBS, Ph3P / CH2Cl2 / 2 h / 0 °C 3: NaN3 / dimethylformamide / 24 h / 60 °C 4: H2 / Lindlar catalyst / methanol / 16 h / 760 Torr / Ambient temperature View Scheme
参考文献
Hunt, Thomas; Atherton-Watson, Hazel C.; Collingwood, Stephen P.; Coote, Kevin J.; Czarnecki, Sarah; Danahay, Henry; Howsham, Catherine; Hunt, Peter; Paisley, Derek; Young, Alice
Bioorganic and Medicinal Chemistry Letters, 2012 , vol. 22, # 8 p. 2877 - 2879