2,6-二甲基-4-氟苯甲腈合成路线 (共 9 条)
反应条件
1: (i) PCl5, (ii) aq. NH3 2: aq. NaOH, Br2 3: (i) aq. HCl, NaNO2, (ii) HPF6 4: H2 / Pd-C 5: (i) NaNO2, aq. HCl, (ii) /BRN= 4652394/ View Scheme
参考文献
Journal of the American Chemical Society, , vol. 89, # 2 p. 390 - 394
反应条件
1: H2 / Pd-C 2: (i) NaNO2, aq. HCl, (ii) /BRN= 4652394/ View Scheme
参考文献
Journal of the American Chemical Society, , vol. 89, # 2 p. 390 - 394
反应条件
1: (i) aq. HCl, NaNO2, (ii) HPF6 2: H2 / Pd-C 3: (i) NaNO2, aq. HCl, (ii) /BRN= 4652394/ View Scheme
参考文献
Journal of the American Chemical Society, , vol. 89, # 2 p. 390 - 394
反应条件
1: aq. NaOH, Br2 2: (i) aq. HCl, NaNO2, (ii) HPF6 3: H2 / Pd-C 4: (i) NaNO2, aq. HCl, (ii) /BRN= 4652394/ View Scheme
参考文献
Journal of the American Chemical Society, , vol. 89, # 2 p. 390 - 394
反应条件
in N,N-dimethyl-formamide Heating;
参考文献
Hu, Yingmo; Ishikawa, Yui; Hirai, Katsuyuki; Tomioka, Hideo
Bulletin of the Chemical Society of Japan, 2001 , vol. 74, # 11 p. 2207 - 2218
反应条件
1: 62 percent / Br2 / CCl4 2: 64 percent / dimethylformamide / Heating View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 74, # 11 p. 2207 - 2218
反应条件
(i) NaNO2, aq. HCl, (ii) /BRN= 4652394/; Multistep reaction;
参考文献
Journal of the American Chemical Society, , vol. 89, # 2 p. 390 - 394
反应条件
1.) diazotization, 2.) Sandmeyer reaction; Yield given. Multistep reaction;
参考文献
Journal of Organic Chemistry, , vol. 53, # 15 p. 3564 - 3568
反应条件
1: (i) H2SO4, (ii) H2O 2: H3PO4 / 150 °C View Scheme
参考文献
Dewar,M.J.S.; Takeuchi,Y.
Journal of the American Chemical Society, 1967 , vol. 89, # 2 p. 390 - 394