2,6-二甲氧基苯甲酸合成路线 (共 118 条)
反应条件
triphenylphosphine; silver carbonate; palladium dichloride in dimethyl sulfoxide; N,N-dimethyl-formamide
T=130°C; 12 h; Inert atmosphere; Reagent/catalystSolvent;
参考文献
Wang, Anwei; Li, Xiujian; Liu, Jidan; Gui, Qingwen; Chen, Xiang; Tan, Ze; Xie, Kai
Synthetic Communications, 2014 , vol. 44, # 2 p. 289 - 295
反应条件
triphenyl-arsane; silver carbonate; palladium dichloride in dimethyl sulfoxide
T=150°C; 6 h;
参考文献
Becht, Jean-Michel; Catala, Cedric; Le Drian, Claude; Wagner, Alain
Organic Letters, 2007 , vol. 9, # 9 p. 1781 - 1783
反应条件
silver carbonate; bis[2-(diphenylphosphino)phenyl] ether; palladium dichloride in dimethyl sulfoxide
T=150°C; 1 h;
参考文献
Becht, Jean-Michel; Le Drian, Claude
Organic Letters, 2008 , vol. 10, # 14 p. 3161 - 3164
反应条件
silver carbonate; palladium dichloride in dimethyl sulfoxide
T=120°C; 1 h;
参考文献
Becht, Jean-Michel; Le Drian, Claude
Organic Letters, 2008 , vol. 10, # 14 p. 3161 - 3164
反应条件
silver carbonate; palladium dichloride in dimethyl sulfoxide
T=120°C; 1 h;
参考文献
Becht, Jean-Michel; Le Drian, Claude
Organic Letters, 2008 , vol. 10, # 14 p. 3161 - 3164
反应条件
silver carbonate; bis[2-(diphenylphosphino)phenyl] ether; palladium dichloride in dimethyl sulfoxide
T=150°C; 1 h;
参考文献
Becht, Jean-Michel; Le Drian, Claude
Organic Letters, 2008 , vol. 10, # 14 p. 3161 - 3164
反应条件
1: (i) SOCl2, (ii) /BRN= 505979/, CH2Cl2, (iii) SOCl2
2: tetrahydrofuran / 3 h / -25 °C
View Scheme
参考文献
Meyers,A.I. et al.
Journal of Organic Chemistry, 1978 , vol. 43, p. 1372 - 1379
反应条件
(i) SOCl2, (ii) /BRN= 505979/, CH2Cl2, (iii) SOCl2; Multistep reaction;
参考文献
Meyers,A.I. et al.
Journal of Organic Chemistry, 1978 , vol. 43, p. 1372 - 1379
反应条件
triphenyl-arsane; silver carbonate; palladium dichloride in dimethyl sulfoxide
T=150°C; 6 h;
参考文献
Becht, Jean-Michel; Catala, Cedric; Le Drian, Claude; Wagner, Alain
Organic Letters, 2007 , vol. 9, # 9 p. 1781 - 1783
反应条件
silver carbonate; copper dichloride; palladium dichloride in tetrahydrofuran
T=110°C; 24 h;
参考文献
Peng, Xuefeng; Shao, Xiang-Feng; Liu, Zhong-Quan
Tetrahedron Letters, 2013 , vol. 54, # 24 p. 3079 - 3081